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ACE72_293.pdf
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The crystal structure of brackebuschite, Pb2Mn3+(VO4)2(OH), was redetermined using single-crystal X-ray diffraction data from a natural sample from Argentina, with improved accuracy and an unambiguous hydrogen-bonding scheme. The structure consists of a cubic closest-packed array of O and Pb atoms, with infinite chains of edge-sharing [Mn3+O6] octahedra decorated by VO4 tetrahedra, held together by irregular [PbOx] polyhedra. The hydroxy group forms a hydrogen bond with a vanadate group, and the structure shows a significant twisting of the chains along [010]. The redetermination improves on previous results, with anisotropic displacement parameters for all non-H atoms and the location of the H atom, and is consistent with Raman spectroscopic data.

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The crystal structure of brackebuschite, Pb2Mn3+(VO4)2(OH), was redetermined using single-crystal X-ray diffraction data from a natural sample from Argentina,...

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  • File Format: PDF
  • File Size: 492 KB
  • Pages: 7
  • Language: EN
  • Total Downloads: 256
  • Last Updated: 16 hours ago

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