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Practicalizing Crystallography Wisdom.pdf

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Preview of Practicalizing Crystallography Wisdom
🔗 Source: waseda-oukakai.gr.jp
📊 Size: 103 KB
👤 Author: Izumi
⬇️ Downloads: 4

Summary

晶析の知恵を実践するには、まずは結晶創りと格闘した40年を経て、晶析工学研究が進歩していることを理解する必要があります。溶液晶析では、結晶は溶解度より高い濃度レベルに調整して、結晶核を生成し、その核を成長させ粗大化させることができます。一方、対象物質が融解する融液晶析では、対象物質を融点以上の温度で融解した後、冷却し過冷却状態にして、核化、成長させることができます。晶析を制御するには、固液平衡、晶析速度（核化、成長）そして収支（物質、個数、熱）をよく理解することが必要になります。工業操作では、結晶品質は速度論的に決まるので、核発生速度や成長速度に影響する因子の関係を定量的に把握しなければならないです。特に、両速度とも、過飽和状態の影響を強く受けるので、装置内の過飽和度の制御が鍵になるです。

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  • File Format: PDF
  • File Size: 103 KB
  • Pages: 2
  • Language: EN
  • Author: Izumi
  • Total Downloads: 4
  • Last Updated: 1 month ago

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