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Supplementary Information PDF (3064K).pdf

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Preview of Supplementary information PDF (3064K)
🔗 Source: rsc.org
📊 Size: 2.92 MB
📄 Pages: 60 pages
⬇️ Downloads: 88

Summary

Researchers developed a general and reusable system for synthesizing 2,5-disubstituted chalcogenophenes using Rongalite in PEG-400. The system allows for the synthesis of selenophenes, thiophenes, and tellurophenes through a simple and efficient procedure. The reaction involves the use of Rongalite, KOH, and elemental chalcogen (selenium, sulfur, or tellurium) in PEG-400, followed by the addition of a 1,3-diyne substrate. The resulting products were isolated and characterized using various spectroscopic techniques, including NMR and HRMS. The system was found to be reusable and scalable, with gram-scale syntheses achieving yields of up to 73%. The developed system provides a valuable tool for the synthesis of chalcogenophenes, which have potential applications in various fields, including materials science and pharmaceuticals.

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Description

Researchers developed a general and reusable system for synthesizing 2,5-disubstituted chalcogenophenes using Rongalite in PEG-400.

Technical Information

  • File Format: PDF
  • File Size: 2.92 MB
  • Pages: 60
  • Language: EN
  • Total Downloads: 88
  • Last Updated: 1 month ago

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